추천 제품
Grade
for GC derivatization
Quality Level
분석
93.0-97.0% (GC)
품질
LiChropur™
구성
trimethylchlorosilane (minor component), 3.0-5.0% GC
반응 적합성
reagent type: derivatization reagent
reaction type: Silylations
기술
gas chromatography (GC): suitable
일반 설명
BSA+TMCS combination, is one of the most commonly used silylating reagents. BSA is readily used for silylating a wide range of functional groups such as non-sterically hindered alcohols, amides, amines, amino acids, carboxylic acids, and enols. TMCS is a silylation catalyst always used with other silylation reagents to increase the reactivity in derivatization of alcohols, alkaloids, amines, biogenic amines, carboxylic acids, phenols, and steroids.
애플리케이션
Learn more in the Product Information
Suitable for the derivatization of α-ketoacids, amines, amino acids, cycloserine, histamine and metabolites, phenylethylamines, phosphatidylserines and tryptamines. BSA+TMCS may be used as a derivatizing reagent for the determination of steryl glycosides in biodiesel using gas chromatography–mass spectrometry.
Suitable for the derivatization of a-ketoacids, amines, amino acids, cycloserine, histamine and metabolites, phenylethylamines, phosphatidylserines and tryptamines.
특징 및 장점
- BSA+TMCS has good solvent properties and can function as a silylation reagent without additional solvents.
- Alternatively, the mixture is very soluble in most commonly used silylation solvents.
- This combination is extremely sensitive to moisture and should be handled under dry conditions.
기타 정보
Powerful silylation mixture with wide applicability
Reagent for trimethylsilyl diglyceride, trimethylsilyl (TMS) and trimethylsilyl oximes.
법적 정보
LiChropur is a trademark of Merck KGaA, Darmstadt, Germany
신호어
Danger
유해 및 위험 성명서
Hazard Classifications
Acute Tox. 4 Oral - Flam. Liq. 2 - Skin Corr. 1A
보충제 위험성
Storage Class Code
3 - Flammable liquids
WGK
WGK 3
Flash Point (°F)
53.6 °F - closed cup
Flash Point (°C)
12 °C - closed cup
개인 보호 장비
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
Removal of pharmaceuticals during drinking water treatment.
Environmental Science & Technology, 36 (17), 3855-3863 (2002)
Biosensors & bioelectronics, 78, 92-99 (2015-11-26)
There are currently no biosensors that are able to reliably detect the process of cancer metastasis. We describe the first label-free real-time ultra-high frequency acoustic wave biosensor prototype capable of detecting the breast and prostate cancer metastasis biomarker, parathyroid hormone-related
Handbook of Analytical Derivatization Reactions, 202-202 (1979)
Journal of Pharmacological Sciences, 62, 1344-1344 (1973)
Z. Anal. Chem., 324, 338-338 (1986)
문서
Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs
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