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55237-U

Supelco

Supel QuE QuEChERS tube

Citrate/Sodium Bicarbonate Tube, pk of 50

동의어(들):

QuEChERS

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About This Item

UNSPSC 코드:
41115712
NACRES:
NB.21

product name

Supel QuE, Citrate/Sodium Bicarbonate Tube, pk of 50

구성

magnesium sulfate, 4 g
sodium bicarbonate, 5 g (Cat. No. S6014)
sodium chloride, 1 g (Cat No. S7653)
sodium citrate dibasic sesquihydrate, 0.5 g (Cat. No. 71635)
sodium citrate tribasic dihydrate, 1 g (Cat. No. S4641)

포장

pk of 50

기술

QuEChERS: suitable

원심분리 튜브 용적

15 mL

응용 분야

food and beverages

분리 기술

ion exchange

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일반 설명

Suitable for extracting ~10 g food/agricultural sample. The citrate is used to buffer the extraction to pH 5.0 - 5.5. At this pH, most acid and base labile pesticides are. The sodium bicarbonate is used to further stablize acid labile pesticides.
Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

법적 정보

Supel is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

13 - Non Combustible Solids

WGK

WGK 1

Flash Point (°F)

Not applicable

Flash Point (°C)

Not applicable


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문서 라이브러리 방문

이미 열람한 고객

Slide 1 of 2

1 of 2

Mohammad Faraji et al.
Food chemistry, 240, 634-641 (2017-09-28)
A QuEChERS based methodology was developed for the simultaneous identification and quantification of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio by liquid chromatography-tandem mass spectrometry for the first time. First, sample extraction was done with MeCN:citrate buffer:NaHCO
Maria Teresa Salles Trevisan et al.
Journal of chromatography. A, 1512, 98-106 (2017-07-20)
An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction
David Moreno-González et al.
Talanta, 128, 299-304 (2014-07-26)
In this study a fast, selective and sensitive multiresidue method based on QuEChERS methodology has been evaluated and validated for the determination of carbamate pesticides, in edible vegetable oils by UHPLC-MS/MS. A new clean-up sorbent, Supel(TM) QuE Z-Sep(+), has been
Lijun Han et al.
Journal of separation science, 39(23), 4592-4602 (2016-11-03)
A novel carbon/zirconia-based material, Supel

프로토콜

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

관련 콘텐츠

QuEChERS는 ‘Quick, Easy, Cheap, Effective, Rugged, Safe’ 시료 정화 방법으로 살충제 분석을 위해 식품과 농산물 시료 전처리에 사용합니다. QuEChERS는 시료 전처리에서 고체상 추출법(SPE) 기술에 기반합니다.

QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.

자사의 과학자팀은 생명 과학, 재료 과학, 화학 합성, 크로마토그래피, 분석 및 기타 많은 영역을 포함한 모든 과학 분야에 경험이 있습니다..

고객지원팀으로 연락바랍니다.