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  • Synthesis and cytotoxic activity of heterocyclic ring-substituted betulinic acid derivatives.

Synthesis and cytotoxic activity of heterocyclic ring-substituted betulinic acid derivatives.

Bioorganic & medicinal chemistry letters (2008-08-30)
Vivek Kumar, Nidhi Rani, Pawan Aggarwal, Vinod K Sanna, Anu T Singh, Manu Jaggi, Narendra Joshi, Pramod K Sharma, Raghuveer Irchhaiya, Anand C Burman
ABSTRACT

A new series of betulinic acid derivatives have been synthesized by introducing heterocyclic ring between C-2 and C-3 positions of betulinic acid. Further modifications were also carried out by reduction of C-20(29) unsaturated bond and substitution of C-28 carboxyl group by ester and amide linkage to enhance the selectivity. Compound 11 resulted in IC(50) of 2.44, 2.5, and 2.7 microg/ml on MIAPaCa, PA-1, and SW620 cancer cell lines, respectively. Compound 38 resulted in IC(50) of 0.67 microg/ml on MIAPaCa cell line.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Betulinic acid, ≥98% (HPLC)
Sigma-Aldrich
Betulinic acid, technical grade, 90%