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Key Documents

1.05582

Supelco

TLC aluminum sheets, Silica gel 60 with concentrating zone 20 x 2.5 cm

pkg of 25 sheets, sheet L × W 20 cm × 20 cm, aluminum support

Synonym(s):

Concentrating Zone TLC Aluminum Sheets

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About This Item

UNSPSC Code:
41115711
NACRES:
NB.21

material

aluminum support
silica gel 60 matrix

Quality Level

feature

binder Organic Polymer
fluorescent indicator: no

packaging

pkg of 25 sheets

technique(s)

thin layer chromatography (TLC): suitable

layer thickness

200 μm

sheet L × W

20 cm × 20 cm

particle size

10-12 μm

pore size

60 Å medium pore diameter

storage temp.

2-30°C

General description

25 Aluminium sheets 20 x 20 cm
These plates allow users to quickly and easily apply any kind of sample, even large volumes of diluted samples. Our concentrating zone plates are based on different adsorption properties of two adsorbents. The first is a large pore concentrating adsorbent where the samples are applied; the second is a selective layer for separation. Regardless of the spots’ shape, size, or position, the sample always concentrates as a narrow band where the two adsorbents overlap and where the separation starts. These plates allow users to quickly and easily apply any kind of sample, even large volumes of diluted samples.

Linkage

Replaces: 5582-7; 5582

Analysis Note

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m²/g
Pore volume (N₂-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 9.7 - 11.7 µm
Layer thickness: 160 - 220 µm
Deviation of layer thickness per plate: ≤ 40 µm
layer thickness concentrating zone: 90 - 140 µm
Fluctuation in the thickness of the concentration zone: ≤ 30 µm
Chromatographic testing:
colour test
hRf-values
- bleu vif organol, colour test, lipophile:
11 - 25
- Ceres Black G, colour test, lipophile: 34 - 48
- ceres Violet brn, colour test, lipophile: 52 - 67
separation number (colourtest, lipophile): ≥ 10.5
Typical value determined on a conditioned sheet
Eluent: toluene (45% rel. humidity)

Certificates of Analysis (COA)

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