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Safety Information

23186

Supelco

Fmoc chloride

≥99.0%, for HPLC derivatization, LiChropur™

Synonym(s):

9-Fluorenylmethoxycarbonyl chloride, 9-Fluorenylmethyl chloroformate, Fmoc-Cl

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About This Item

Empirical Formula (Hill Notation):
C15H11ClO2
CAS Number:
28920-43-6
Molecular Weight:
258.70
Beilstein:
2279177
EC Number:
249-313-6
MDL number:
MFCD00001138
UNSPSC Code:
12000000
PubChem Substance ID:
329752393
NACRES:
NA.22

Product Name

Fmoc chloride, for HPLC derivatization, LiChropur™, ≥99.0% (HPLC)

grade

for HPLC derivatization

Quality Level

100

Assay

≥99.0% (HPLC)

form

solid

quality

LiChropur™

technique(s)

HPLC: suitable

mp

61-64 °C
62-64 °C (lit.)

storage temp.

2-8°C

SMILES string

ClC(=O)OCC1c2ccccc2-c3ccccc13

InChI

1S/C15H11ClO2/c16-15(17)18-9-14-12-7-3-1-5-10(12)11-6-2-4-8-13(11)14/h1-8,14H,9H2

InChI key

IRXSLJNXXZKURP-UHFFFAOYSA-N

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General description

Fmoc chloride is a derivatizing agent.

Application

Fmoc chloride may be used as derivatizing reagent in pre-column derivatization of the biogenic amines, resolved using HPLC technique.
Reagent for derivatizing amino acids for HPLC amino acid analysis and for preparing N-Fmoc amino acids for solid-phase peptide synthesis.

Other Notes

Reagent for precolumn derivatization of amines for HPLC and fluorescent detection (abs.: 265 nm, em.: 315 nm); Used for capillary electrophoresis

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Legal Information

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

Pictograms

Corrosion
GHS05

Signal Word

Danger

Hazard Statements

H314

Hazard Classifications

Eye Dam. 1 - Skin Corr. 1B

Supplementary Hazards

EUH029

Storage Class Code

8A - Combustible corrosive hazardous materials

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

Regulatory Listings

Regulatory Listings are mainly provided for chemical products. Only limited information can be provided here for non-chemical products. No entry means none of the components are listed. It is the user’s obligation to ensure the safe and legal use of the product.

JAN Code

23186-5G:
23186-BULK:
23186-1G:
23186-VAR:

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Certificates of Analysis (COA)

Lot/Batch Number
BCCM7018
BCCM6531
BCCM2032
BCCK2354
BCCK2058

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K C Chan et al.
Journal of chromatography. A, 653(1), 93-97 (1993-10-29)
Laser-induced fluorescence (LIF) was applied to the detection of 9-fluorenylmethyl chloroformate (FMOC-Cl) derivatized amino acids separated by capillary electrophoresis. Fluorescence excitation was provided by a pulsed, KrF laser operating at 248 nm. A limit of detection of 5 x 10(-10)
J.V. Sancho et al.
Journal of Chromatography A, 678, 59-59 (1994)
J. Kirschbaum et al.
Journal of Chromatography A, 661, 193-193 (1994)
S. Einarsson et al.
Analytical Chemistry, 58, 1638-1638 (1986)
Ingrid Freuze et al.
Journal of chromatography. A, 1175(2), 197-206 (2007-11-21)
Experimental and theoretical influence of multivalent cations on the analysis of glyphosate and aminomethyl phosphonic acid (AMPA) was studied in pure water and in one surface water. The procedure chosen, based on derivatization with FMOC-Cl, HPLC separation, and fluorescence detection
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