GC Analysis of Impurities in Propylene on Alumina Chloride PLOT
CONDITIONS
column
Alumina chloride PLOT, 50 m x 0.53 mm I.D. (28329-U)
oven
35 °C (2.5 min), 5 °C/min to 150 °C (4.5 min)
inj. temp.
200 °C
detector
FID, 230 °C
carrier gas
helium, 3.0 mL/min
injection
10 μL, direct using a sampling valve, 150 °C
sample
18-component C1-C5 hydrocarbon standard in nitrogen, spiked into propylene