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Merck

54341-U

Supelclean EZ-POP NP solid phase extraction (SPE) Tube

volume 12 mL, pkg of 20

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제품정보 (DICE 배송 시 비용 별도)

UNSPSC 코드:
41115712
NACRES:
NB.21
기술 서비스
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제품 이름

Supelclean EZ-POP NP, volume 12 mL, pkg of 20

material

polypropylene tube

Quality Level

제품 라인

Supelclean

구성

bed A, 1.25 g (Supelclean LC-Florisil®)
bed b, 1.25 g (Z-Sep/C18)

포장

pkg of 20

기술

solid phase extraction (SPE): suitable

용적

12 mL

기질 활성군

C18 bonding phase
florisil bonding phase
zirconia bonding phase

응용 분야

food and beverages

일반 설명

Retention Mechanisms: Lipid matrix is retained via normal phase, hydrophobic, and Lewis acid-Lewis base interactions
Sample Matrix Compatibility: Oils

  • Dual layer SPE that contains both LC-Florisil® (upper layer) and Z-Sep/C18 (lower layer) SPE sorbents, separated by a PE frit.
  • Developed to offer superior cleanup when analyzing non-polar persistent organic pollutants (POPs) from oil matrices.
  • Fatty matrix is preferentially retained by the cartridge, while non-polar POPs are washed through using acetonitrile.

This multi-bed solid phase extraction (SPE) cartridge was designed for the extraction of non-polar persistent organic pollutants (POPs), specifically heavy and light polynuclear aromatic hydrocarbons (PAHs), from edible oil matrices such as olive and corn oil. Fatty matrix is preferentially retained by the cartridge while PAHs are washed through using acetonitrile. The resulting extract is suitable for either GC-MS or HPLC-FLD analysis. The top layer of the SPE cartridge consists of Florisil®, a polar adsorption media that interacts with polar functional groups such as acids and alcohols. The bottom layer is comprised of a mixture of Discovery® DSC-18 and Z-Sep sorbents. C18 binds fatty matrix through hydrophobic interaction. Z-Sep, a zirconia coated silica, acts as a Lewis acid, interacting with the oxygen within OH and COOH groups found in fatty acids and mono and diacylglycerols.

법적 정보

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Florisil is a registered trademark of U.S. Silica Company
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point (°F)

Not applicable

Flash Point (°C)

Not applicable


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시험 성적서(COA)

Lot/Batch Number

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특정 버전이 필요한 경우 로트 번호나 배치 번호로 특정 인증서를 찾을 수 있습니다.

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문서 라이브러리에서 최근에 구매한 제품에 대한 문서를 찾아보세요.

문서 라이브러리 방문

Analysis of Polynuclear Aromatic Hydrocarbons in Olive Oil After Solid Phase Extraction Using a Dual-Layer Sorbent Cartridge Followed by HPLC Fluorescence Analysis
Stenerson, K.K., et al.
Journal of Agricultural and Food Chemistry (2015)

문서

Compare PAH determination in olive oil: traditional GB 5009.265-2021 method vs. faster, simpler SPE with Supelclean EZ-POP NP; both meet criteria.

프로토콜

Paprika spice's PAH contamination risk due to environmental exposure highlights food safety concerns.

관련 콘텐츠

Solid phase extraction purifies samples for chromatographic analysis, improving data quality and protecting analytical columns.

Solid phase extraction purifies samples for chromatographic analysis, improving data quality and protecting analytical columns.

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