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  • B-(3,3-difluoroallyl)diisopinocampheylborane for the enantioselective fluoroallylboration of aldehydes.

B-(3,3-difluoroallyl)diisopinocampheylborane for the enantioselective fluoroallylboration of aldehydes.

The Journal of organic chemistry (2012-09-15)
P Veeraraghavan Ramachandran, Agnieszka Tafelska-Kaczmarek, Anamitra Chatterjee
ABSTRACT

The fluoroallylboration of aldehydes with B-(3,3-difluoroallyl)diisopinocampheylborane, which was prepared via the hydroboration of 1,1-difluoroallene, provides chiral 2,2-gem-difluorinated homoallylic alcohols in good yields and 91-97% ee.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Allyl alcohol, ≥98.5%
Sigma-Aldrich
Allyl alcohol, ≥98.5%
Sigma-Aldrich
Allyl alcohol, ≥99%