794-0441

GCによる塩素系殺虫剤の分析、SPB^®-5 、SPME処理 、100 μm PDMS使用

suitable for GC, application for SPME

特性

• テクニック: gas chromatography (GC): suitable; solid phase microextraction (SPME): suitable
• 試験パラメータ: sample/matrix: 200 ppt each in 2 mL water; SPME fiber: polydimethylsiloxane, 100 μm (57300-U); extraction: 15 min immersed in water with rapid stirring; column: SPB-5, 15 m × 0.20 mm I.D., 0.20 μm (24165-U); oven: 120 °C (1 min) to 180 °C at 30 °C/min, then to 290 °C at 10 °C/min; inj. temp.: 260 °C (splitless - closed 3 min); detector: ECD, 300 °C; carrier gas: helium, 37 cm/sec (set at 120 °C)
• 適合性: application for SPME
• アプリケーション: environmental; food and beverages

詳細

法的情報

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

アナライト

4,4′-DDD, PESTANAL^®, analytical standard
Endrin aldehyde
Aldrin
Dieldrin
α-BHC
Endosulfan sulfate
Endrin ketone
α-Chlordane
γ-Chlordane
δ-BHC
Decachlorobiphenyl
4,4′-DDT
Methoxychlor
Heptachlor
γ-BHC, certified reference material, 1000 μg/mL in methanol
Endrin
β-BHC
1,1-Dichloro-2,2-bis(4-chlorophenyl)ethene
Heptachlor epoxide, PESTANAL^®, analytical standard, isomer B
すべて表示 (19)