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Merck
모든 사진(2)

주요 문서

1.06018

Supelco

Methanol

≥99.8% (GC), HPLC grade, suitable for HPLC, LiChrosolv®

동의어(들):

MeOH, Hydroxymethane, Carbinol, Methyl alcohol

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About This Item

Linear Formula:
CH3OH
CAS Number:
Molecular Weight:
32.04
Beilstein:
1098229
MDL number:
UNSPSC 코드:
12191502
EC 인덱스 번호:
200-659-6
NACRES:
NA.03

product name

Methanol, for liquid chromatography LiChrosolv®

Grade

HPLC grade

Quality Level

vapor density

1.11 (vs air)

vapor pressure

128 hPa ( 20 °C)
410 mmHg ( 50 °C)
97.68 mmHg ( 20 °C)

제품 라인

LiChrosolv®

grade

isocratic

분석

≥99.8% (GC)

형태

liquid

autoignition temp.

725 °F

효능

5628 mg/kg LD50, oral (Rat)
17100 mg/kg LD50, skin (Rabbit)

expl. lim.

36 %

기술

HPLC: suitable

불순물

≤0.0002 meq/g Acidity
≤0.0002 meq/g Alkalinity
≤0.03% Water

증발 잔류물

≤3.0 mg/L

색상

APHA: ≤10

투과

225 nm, ≥50%
240 nm, ≥80%
265 nm, ≥98%

refractive index

n20/D 1.329 (lit.)

kinematic viscosity

0.54-0.59 cSt(20 °C)

bp

64.7 °C (lit.)

mp

−98 °C (lit.)

전이 온도

flash point 9.7 °C

density

0.791 g/mL at 25 °C (lit.)

형식

neat

저장 온도

2-30°C

SMILES string

CO

InChI

1S/CH4O/c1-2/h2H,1H3

InChI key

OKKJLVBELUTLKV-UHFFFAOYSA-N

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일반 설명

LiChrosolv® solvents exhibit high degree of UV transmittance, low particle count, low acidity and alkalinity and low evaporation residue level. This makes them ideal for reproducible separations.

애플리케이션

Intended for HPLC and UHPLC-MS applications.
Featured in method development of:
  • Benazepril - USP Method Benazepril RS
  • Betamethasone - USP Method Betamethasone Valerate Assay
  • Irbesartan - USP Method Irbesartan Assay
  • Lamivudine - USP Method Lamivudine RS
  • Lansoprazole - USP Method Lansoprazole RS
  • Levofloxacin - USP Method Levofloxacin RS - USP Method Levofloxacin Assay
  • Nifedipine - USP Method Nifedipine RS - USP Method Nifedipine Assay
  • Pharmacopoeia Monograph Methods - HPLC and UHPLC methods for Regulated Drug Analysis
  • Pioglitazone - USP Method Pioglitazone HCl RS - USP Method Pioglitazone HCl Assay

특징 및 장점

  • suitability tested and specified for UHPLC-MS and UHPLC-UV: for analytical flexibility
  • specified quality in positive and negative in positive and negative electrospray ionization (ESI) and atmospheric-pressure chemical ionization-mass spectrometry (APCI-MS) for lowest detection limits and confidence in analyses for all important MS modes (test 1)
    —ESI/APCI (+) < 2 ppb
    —ESI/APCI (-) < 10 ppb
  • lowest impurity profile: for interference-free baselines (test 2)
  • microfiltered through 0.2 μm filter (test 3) to provide:
    —A long lifespan to filters and mechanical parts of HPLC systems
    ––reduced risk of column clogging
  • packaged in borosilicate glass bottles for minimized metal ion contaminations
  • lowest levels of trace metal impurities for a minimum metal ion adduct formation
    —<5 ppb
  • lowest level of polyethylene glycol (PEG) impurities in UHPLC-MS solvent lineup (PEG S/N signal-to-noise-ratio < 50)

제조 메모

Product filtered through a 0.2 μm filter

분석 메모

Evaporation Number: 1.9
Purity (GC): ≥ 99.8 %
Identity (IR): conforms
Evaporation residue: ≤ 3.0 mg/l
Water: ≤ 0.03 %
Color: ≤ 10 Hazen
Acidity: ≤ 0.0002 meq/g
Alkalinity: ≤ 0.0002 meq/g
Transmission (at 225 nm): ≥ 50 %
Transmission (at 240 nm): ≥ 80 %
Transmission (from 265 nm): ≥ 98 %
Filtered by 0.2 µm filter

기타 정보

Explore various lab safety accessories and equipment for safe handling of solvents to increase your safety level from the first usage.

법적 정보

LICHROSOLV is a registered trademark of Merck KGaA, Darmstadt, Germany

픽토그램

FlameSkull and crossbonesHealth hazard

신호어

Danger

유해 및 위험 성명서

Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Flam. Liq. 2 - STOT SE 1

표적 기관

Eyes,Central nervous system

Storage Class Code

3 - Flammable liquids

WGK

WGK 2

Flash Point (°F)

49.5 °F - closed cup

Flash Point (°C)

9.7 °C - closed cup


시험 성적서(COA)

제품의 로트/배치 번호를 입력하여 시험 성적서(COA)을 검색하십시오. 로트 및 배치 번호는 제품 라벨에 있는 ‘로트’ 또는 ‘배치’라는 용어 뒤에서 찾을 수 있습니다.

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이미 열람한 고객

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문서

An HPTLC method for rapid urea detection in milk using a TLC plate scanner and Silica Gel 60 F254 HPTLC plate.

HPTLC separation followed by UV detection of the bitter acid content in various hop samples.

HPLC-DAD method on Ascentis® Express C8 column analyzes safinamide purity and related impurities meeting system suitability criteria.

This application note describes the HPTLC-based identification of fixed oils using octadecyl silyl silica gel as the coating substance, following USP 43 NF 38 monograph method containing USP general chapter <202>.

모두 보기

프로토콜

HPTLC was used to analyze caffeine in coffee. Filtration of coffee through a PTFE syringe filter was the only sample preparation. Quantitation was conducted with a TLC scanner.

GB method with Ascentis® Express C30 column achieves baseline resolution for Vitamin A and E critical pair.

In the present study we demonstrate compliance of silica gel 60 F254 HPTLC plates with USP requirements, and how HPTLC plates are suitable for the Sildenafil citrate-Limit of Imidazole test.

Folic acid vs. folate differences and biological activities; implications in fortified foods and supplements for human health.

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