G003776

GC Analysis of Organophosphorus Pesticides (OP-Pest) on SLB^®-5ms after SPME using 60 μm Carbowax^® Fiber

application for SPME, suitable for GC

속성

• 기술: gas chromatography (GC): suitable; solid phase microextraction (SPME): suitable
• 검사 파라미터: sample/matrix: Organophosphate pesticides at 10ppb in 0.2M phasphate buffer, pH 7, with 25% NaCl, 9mL in 10 mL vial; SPME fiber: 60 μm Carbowax(PEG) (57354-U); extraction: 30 min. direct immersion with agitation using CombiPal autosampler; desorption process: 2 min at 250°C, splitless for 0.75 min then opened; column: SLB-5ms 30 m x 0.25mm I.D., 0.5 μm film; oven: 60°C(1 min) to 215°C @ 20°C/min to 290°C @ 6°C/min (1 min); inj. temp.: Splitless/split with 0.75mm ID liner and Merlin Microseal; detector: ITMS m/z=50-326 @ 0.6 μsec per scan, transfer line 310°C; carrier gas: Helium, 1mL/min constant flow
• 적합성: application for SPME
• 응용 분야: agriculture; chemicals and industrial polymers; environmental; food and beverages

설명

법적 정보

Carbowax is a registered trademark of Union Carbide

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

분석물

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