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57221-U

Supelco

Discovery® DSC-SCX SPE Bulk Packing

pkg of 100 g

NACRES:
NB.21

packaging

pkg of 100 g

Quality Level

technique(s)

solid phase extraction (SPE): suitable

matrix active group

sulfonic acid bonding

application(s)

food and beverages

separation technique

ion exchange

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57228-U52688-U52689-U
matrix active group

sulfonic acid bonding

matrix active group

carboxypropyl bonding

matrix active group

sulfonic acid bonding

matrix active group

sulfonic acid bonding

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

separation technique

ion exchange

separation technique

ion exchange

separation technique

ion exchange

separation technique

ion exchange

technique(s)

solid phase extraction (SPE): suitable

technique(s)

solid phase extraction (SPE): suitable

technique(s)

solid phase extraction (SPE): suitable

technique(s)

solid phase extraction (SPE): suitable

General description

Retention Mechanism: Cation exchange
Sample Matrix Compatibility: Organic or aqueous solutions

  • A polymerically bonded, benzene sulfonic acid functional group, pKa (< 1.0)
  • Counter ion is H+
  • Silica support allows for use with very organic solvents (no shrinking/swelling)
  • Excellent capacity (0.8 meq/g) for cleaning up solution phase combinatorial chemistry reactions (removing target molecules from reaction by-products and excess reagents)
  • The presence of the benzene ring offers some mixed-mode capabilities (hydrophobic interactions) that should be considered when extracting cations from aqueous matrices

Legal Information

Discovery is a registered trademark of Sigma-Aldrich Co. LLC

Pictograms

CorrosionExclamation mark

Signal Word

Danger

Hazard Statements

Hazard Classifications

Aquatic Chronic 3 - Eye Dam. 1 - Skin Corr. 1A - Skin Sens. 1

Storage Class Code

8A - Combustible, corrosive hazardous materials

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


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Protocols

Analysis of Melamine in Milk

Melamine was extracted from milk using Supelco® Discovery® DSC-SCX SPE tubes. Analysis was performed by HPLC, using an Ascentis® Express HILIC column.

Solid Phase Extraction: Normal Phase Methodology

Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

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