G004844
GC Analysis of Resveratrol in Red Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber
suitable for GC, application for SPME
technique(s)
gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable
test parameters
sample/matrix: 3 mL of red wine (California merlot) diluted 3:1 in 12% ethanol:water
SPME fiber: 85 μm polyacrylate FS 23 gauge auto (57294-U)
SPME fiber: 85 μm polyacrylate FS 24gauge auto (57305)
SPME fiber: 85 μm polyacrylate FS 24gauge manual (57304)
extraction: immersion for 15 min at room temperature while stirring at 400 rpm, fiber gently blotted with a Kimwipe to remove excess water, (then derivatization by immersion in a 4 mL vial containing 5 μL of Sylon-BFT (fresh vial for each analysis than was allowed to equilabrate 60-90 minutes prior to use) for 20 min)
desorption process: 280 °C for 2 min
column: SLB-5ms; 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 100 °C (1 min), 10 °C/min to 325 °C (3 min)
MSD interface: 325 °C
scan range: m/z 40-450
carrier gas: helium, 1 mL/min, constant
liner: 0.75 mm I.D., SPME
suitability
application for SPME
application(s)
food and beverages
Legal Information
SPME fiber
accessory
analytical column
related product
standard
Certificates of Analysis (COA)
Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.
Already Own This Product?
Find documentation for the products that you have recently purchased in the Document Library.
Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.
Contact Technical Service