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  • [Study on chemical constituents from ethyl acetate extract of Myricaria bracteata].

[Study on chemical constituents from ethyl acetate extract of Myricaria bracteata].

Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica (2011-08-04)
Ying Zhang, Yi Yuan, Baosong Cui, Shuai Li
ABSTRACT

To study the chemical constituents from the ethyl acetate extract of Myricaria bracteata. The chemical constituents were isolated and purified by chromatographic techniques, and their structures were identified by physical characters and spectroscopic analysis. Sixteen compounds were isolated from the ethyl acetate portion of the 95% ethanolic extract of Myricaria bracteata, and identified as myricarin (1), myricarin B (2), 3alpha-hydroxytaraxer-14-en-28-oic acid (3), myricadiol (4), trans-ferulic acid 22-hydroxydocosanoic acid ester (5), docosyl-3, 4-dihydroxy-trans-cinnamate (6), dillenetin (7), 3, 5, 4'-trihydroxy-7-methoxyflavone (8), 3, 5, 4'-trihydroxy-7, 3'-dimethoxyflavone (9), methyl 3, 5-dihydroxy-4-methoxybenzoate (10), 3-hydroxy-4-methoxy cinnamic acid (11), sinapaldehyde (12), vanillin (13), syringaldehyde (14), 3, 3', 4'-trimethoxyellagic acid (15), methyl p-hyroxybenzoate (16). Compounds 5, 6, 12-16 were isolated from the genus Myricaria for the fist time, all of the compounds were isolated from this plant for the fist time, except for 8 and 9.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
3-Hydroxy-4-methoxycinnamic acid, predominantly trans, 97%
Sigma-Aldrich
Syringaldehyde, ≥98%, FG
Sigma-Aldrich
Syringaldehyde, 98%