GC Analysis of Basic Drugs on SLB®-5ms
Materials
analytical column
Product No.
Description
Pricing
CONDITIONS
column
SLB-5ms, 30 m x 0.25 mm I.D., 0.50 μm (28473-U)
oven
45 °C (2.0 min), 30 °C/min to 110 °C (1.0 min), 15 °C/min to 200 °C (1.0 min), 4 °C/min to 310 °C (5.0 min)
inj. temp.
250 °C
MSD interface
330 °C
scan range
m/z = 40-450
carrier gas
helium, 0.7 mL/min constant
injection
0.5 μL, pulsed splitless, 30 psi (0.20 min), purge on (1.50 min), purge flow (50.0 mL/min)
liner
2 mm I.D., straight
sample
drugs of abuse standard diluted to 100 ppm in methanol
Description
Legal Information
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany