US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SPB®-608
Materials
Analytical column
Product No.
Description
Pricing
accessory
Product No.
Description
Pricing
Wheaton wide-mouth bottle
amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 eaguard column
recommended
Product No.
Description
Pricing
required but not provided
standard
Product No.
Description
Pricing
Pesticide Surrogate Spike Mix
certified reference material, TraceCERT®, 200 μg/mL each component in acetone, ampule of 1 mLEPA CLP Organochlorine Pesticide MIx
certified reference material, 2000 μg/mL each component in hexane: toluene (1:1), ampule of 1 mLCONDITIONS
column
SPB-608, 30 m x 0.25 mm I.D., 0.25 μm (24103-U)
oven
100 °C (2 min), 15 °C/min to 300 °C (5 min)
inj. temp.
250 °C
detector
ECD, 300 °C
carrier gas
helium, 0.9 ml/min, constant flow
injection
2.0 μL, splitless (0.75 min)
liner
4 mm I.D. single taper
sample
chlorinated pesticide standard (cat. No. 46845-U), 50 ppb in methylene chloride
Description
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany