GC Analysis of a 17-Component Dioxin Congener Mix on SLB^®-5ms (15 m x 0.10 mm I.D., 0.10 μm), Fast GC Analysis

column

SLB-5ms, 15 m x 0.10 mm I.D., 0.10 μm (28466-U)

oven

150 °C (1 min), 35 °C/min to 340 °C (1 min)

inj. temp.

250 °C

detector

ECD, 340 °C

carrier gas

hydrogen, 45 cm/sec, constant

injection

1 μL splitless (1 min)

liner

4 mm I.D., single taper

sample

17-component 2,3,7,8-substituted dioxin standard, 100-500 ppb in n-nonane