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GC Analysis of cis/trans Limonene Oxide Enantiomers on Astec® CHIRALDEX B-PH

GC Analysis of cis/trans Limonene Oxide Enantiomers on Astec® CHIRALDEX™ B-PH suitable for GC

Materials

analytical column

Product No.
Description
Pricing

Astec® CHIRALDEX B-PH Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

standard

Product No.
Description
Pricing

(R)-(+)-Limonene

analytical standard

(R)-(+)-Limonene

technical, ~90% (sum of enantiomers, GC)

(S)-(−)-Limonene

analytical standard

(S)-(−)-Limonene

96%

(R)-(+)-Limonene

97%

(S)-(−)-Limonene

≥95%, FG

(R)-(+)-Limonene

≥93%

CONDITIONS

column

Astec CHIRALDEX B-PH, 30 m x 0.25 mm I.D., 0.12 μm (71023AST)

oven

90 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 24 psi

injection

1 μL, 80:1 split

sample

3 mg/mL in methylene chloride
peak 1: d-cis or d-trans limonene oxide
peak 2: l-cis and trans limonene oxide
peak 3: d-trans or d-cis limonene oxide

Description

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC