LC/MS Analysis of Antipsychotic Drugs on Ascentis® Express RP Amide
Materials
Analytical column
Product No.
Description
Pricing
Standard
Product No.
Description
Pricing
Bupropion hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®(±)-Hydroxybupropion solution
1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®9-Hydroxyrisperidone solution
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Ascentis Express RP Amide, 10 cm x 2.1 mm I.D., 2.7 μm particles (53913-U)
mobile phase
[A] 5 mM ammonium formate water; [B] 5mM ammonium formate in 95:5 (v/v) methanol:water
gradient
held at 35% B for 0.5 min; 35 to 85% B in 5.5 min; held at 85% B for 1 min
flow rate
0.3 mL/min
pressure
4641 psi (320 bar)
column temp.
35 °C
detector
ESI(+), m/z 100-1000
injection
1 μL
sample
200 ng/mL in waler
Description
Legal Information
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany