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167398

Sigma-Aldrich

tert-Butyl carbamate

98%

동의어(들):

Boc-amide

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모든 사진(3)

About This Item

Linear Formula:
NH2COOC(CH3)3
CAS Number:
4248-19-5
Molecular Weight:
117.15
Beilstein:
1744500
EC Number:
224-209-3
MDL number:
MFCD00007962
UNSPSC 코드:
12352100
PubChem Substance ID:
24850207
NACRES:
NA.22

분석

98%

형태

solid

mp

105-108 °C (lit.)

SMILES string

CC(C)(C)OC(N)=O

InChI

1S/C5H11NO2/c1-5(2,3)8-4(6)7/h1-3H3,(H2,6,7)

InChI key

LFKDJXLFVYVEFG-UHFFFAOYSA-N

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일반 설명

Palladium-catalyzed cross-coupling reaction of tert-butyl carbamate with various aryl(Het) halides with Cs2CO3 as base in 1,4-dioxane (solvent) has been investigated.

애플리케이션

tert-Butyl carbamate was used in palladium-catalyzed synthesis of N-Boc-protected anilines. It was used in the synthesis of tetrasubstituted pyrroles, functionalized with ester or ketone groups at C-3 position.

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point (°F)

Not applicable

Flash Point (°C)

Not applicable

개인 보호 장비

Eyeshields, Gloves, type N95 (US)

시험 성적서(COA)

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The scope of Pd-catalyzed synthesis of N-Boc-protected anilines from aryl bromides and commercially available tert-butyl carbamate is described. For the first time, this process can be conducted at room temperature (17-22 degrees C) using a combination of Pd(2)dba(3).CHCl(3) and a
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Journal of Heterocyclic Chemistry, 47(1), 233-236 (2010)
Pd-catalyzed amidation of aryl (Het) halides with< i> tert</i>-butyl carbamate.
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