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Sigma-Aldrich

KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2

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About This Item

UNSPSC 코드:
12161600
NACRES:
NA.21

반응 적합성

reagent type: catalyst
core: palladium
reaction type: Miyaura Borylation Reaction

작용기

phosphine

일반 설명

The KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit enables chemists to quickly and efficiently screen reaction conditions for Pd catalyzed Miyaura borylation reactions. Quick identification of optimal conditions allows faster scale-up of the desired synthetic transformation. All required chemicals come pre-weighed for ease of use. A step-by-step user guide and experimental excel sheets are available for download to facilitate the process.

애플리케이션

Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:

  • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
  • 4 x 4 mL reaction vials with pre-weighed KOAc
  • Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
  • 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
  • 4 stir bars for substrate stock solution vials.
  • 1 internal standard.
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

특징 및 장점

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reactions in parallel.
  • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

법적 정보

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

키트 구성품 역시 별도로 이용 가능함

제품 번호
설명
SDS

  • 764175P(Cy3) Pd G3, 97%SDS

  • 791733Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%SDS

  • 804274XPhos Pd G4, 95%SDS

  • 804282SPhos Pd G4SDS

  • 804290RuPhos Pd G4SDS

  • 804975DTBPF-Pd-G3SDS

  • 900349cataCXium Pd G4SDS

  • 900522Toluene, anhydrous, ZerO2®, 99.8%SDS

  • 900631Ethylene glycol, anhydrous, ZerO2®, 99.8%SDS

  • 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8%SDS

  • 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%SDS

  • 9006391-Butanol, anhydrous, ZerO2®, 99.8%SDS

  • 900641Methanol, anhydrous, ZerO2®, 99.8%SDS

  • 900644Acetonitrile, anhydrous, ZerO2®, 99.8%SDS

  • 900690N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5%SDS

  • 221171Pinacol, 98%SDS

  • 473294Bis(pinacolato)diboron, 99%SDS

  • 754242Tetrahydroxydiboron, 95%SDS

  • B34656Biphenyl, ReagentPlus®, 99.5%SDS

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mmSDS

  • Z742110KitAlysis 24-well reaction block replacement filmSDS

모두 보기 (21)

신호어

Danger

Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1 - STOT SE 3

표적 기관

Central nervous system, Eyes,Central nervous system, Kidney, Respiratory system

보충제 위험성

Storage Class Code

3 - Flammable liquids

Flash Point (°F)

1.4 °F

Flash Point (°C)

-17 °C


시험 성적서(COA)

제품의 로트/배치 번호를 입력하여 시험 성적서(COA)을 검색하십시오. 로트 및 배치 번호는 제품 라벨에 있는 ‘로트’ 또는 ‘배치’라는 용어 뒤에서 찾을 수 있습니다.

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문서 라이브러리 방문

문서

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

프로토콜

Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.

관련 콘텐츠

유기합성에서 화학 반응 디자인과 최적화는 반응 파라미터를 정밀하게 변경하여 표적 분자를 향한 경로 발견에서 최적의 결과 달성을 목표로 합니다.

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

자사의 과학자팀은 생명 과학, 재료 과학, 화학 합성, 크로마토그래피, 분석 및 기타 많은 영역을 포함한 모든 과학 분야에 경험이 있습니다..

고객지원팀으로 연락바랍니다.