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KITALYSIS-RCM

Sigma-Aldrich

KitAlysis™ High-Throughput Medium (5, 6, 7) Ring Closing Metathesis Reaction Screening Kit - Pack of 2

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About This Item

UNSPSC 코드:
12161600
NACRES:
NA.22

반응 적합성

core: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling

저장 온도

2-8°C

관련 카테고리

애플리케이션

Screening kit for ring closing metathesis. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.

Step-by-Step Guide for Ring Closing Metathesis/Cross Metathesis Reaction Screening Kit

Downloadable experimental excel file

Each kit contains 2 customizable screening sets that include the following components:
  • 6x4 pre-weighed catalysts in glass microvials loaded with stir bars and topped with cap mat.
  • 2 (2 mL) ampules each of of ClPh, PhMe, i-PrOAc, Me-THF, and TFA.
  • 1 KitAlysis 24-well reaction block replacement film.
  • 4 empty substrate stock solution reaction vials with stir bars.
  • 1 internal standard.
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

특징 및 장점

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reaction in parallel.
  • 20 μmol reactions with 1 μmol catalyst (5 mol%), 0.2 M concentration, and optional TFA additive.
  • Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.

법적 정보

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

키트 구성품 전용

제품 번호
설명
  • SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

키트 구성품 역시 별도로 이용 가능함

제품 번호
설명
SDS
  • 569747Grubbs Catalyst® M204, Umicore 3 µmolSDS
  • 569755Hoveyda-Grubbs Catalyst® M720, Umicore, 97% 3 µmolSDS
  • 579726Grubbs Catalyst® M102, Umicore, 97% 3 µmolSDS
  • 682365Grubbs Catalyst® M207, Umicore 3 µmolSDS
  • 682373Hoveyda-Grubbs Catalyst® M721, Umicore 3 µmolSDS
  • 729345Hoveyda-Grubbs Catalyst® M722, Umicore 3 µmolSDS
  • 900519Isopropyl acetate, anhydrous, ZerO2®, ≥99.6% 8 mLSDS
  • 9005202-Methyltetrahydrofuran, anhydrous, contains 250 ppm BHT as stabilizer, ZerO2®, ≥99.0% 8 mLSDS
  • 900521Chlorobenzene, anhydrous, ZerO2®, 99.8% 8 mLSDS
  • 900522Toluene, anhydrous, ZerO2®, 99.8% 8 mLSDS
  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EASDS
모두 보기 (11)

관련 제품

제품 번호
설명
가격

추천

제품 번호
설명
가격

신호어

Danger

Hazard Classifications

Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3

표적 기관

Central nervous system, Respiratory system

보충제 위험성

EUH019

Storage Class Code

3 - Flammable liquids

WGK

WGK 3

시험 성적서(COA)

제품의 로트/배치 번호를 입력하여 시험 성적서(COA)을 검색하십시오. 로트 및 배치 번호는 제품 라벨에 있는 ‘로트’ 또는 ‘배치’라는 용어 뒤에서 찾을 수 있습니다.

이 제품을 이미 가지고 계십니까?

문서 라이브러리에서 최근에 구매한 제품에 대한 문서를 찾아보세요.

문서 라이브러리 방문

Scientist-Led High-Throughput Experimentation (HTE) and Its Utility in Academia and Industry.
Schmink JR, et al.
Aldrichimica Acta, 46, 71-80 (2013)
Karl D Collins et al.
Nature chemistry, 6(10), 859-871 (2014-09-23)
New organic reactivity has often been discovered by happenstance. Several recent research efforts have attempted to leverage this to discover new reactions. In this Review, we attempt to unify reported approaches to reaction discovery on the basis of the practical
High-Throughput Experimentation in Catalysis and Materials Science.
Gordillo A, et al.
Ullmann's Encyclopedia of Industrial Chemistry (2014)
Spencer D Dreher et al.
Journal of the American Chemical Society, 130(29), 9257-9259 (2008-06-28)
Microscale parallel experimentation was used to discover three catalyst systems capable of coupling secondary organotrifluoroborates with sterically and electronically demanding aryl chlorides and bromides. The ensuing results represent the first comprehensive study of alkylboron coupling to aryl chlorides and, in

문서

KitAlysis™ High-Throughput Screening Platform

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

프로토콜

Catalyst Screening & TLC-MS for Reaction Analysis

Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.

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유기합성에서 화학 반응 디자인과 최적화는 반응 파라미터를 정밀하게 변경하여 표적 분자를 향한 경로 발견에서 최적의 결과 달성을 목표로 합니다.

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Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

자사의 과학자팀은 생명 과학, 재료 과학, 화학 합성, 크로마토그래피, 분석 및 기타 많은 영역을 포함한 모든 과학 분야에 경험이 있습니다..

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