MilliporeSigma
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55174-U

Supelco

Supel QuE

PSA/ENVI-Carb (EN) Cleanup Tube 1, pack of 100, suitable for EN 15662:2008 per BS

Synonym(s):
QuEChERS
NACRES:
NB.21

Agency

suitable for BS EN 15662:2008

Quality Level

composition

magnesium sulfate, 150 mg
Supelclean ENVI-Carb, 2.5 mg
Supelclean PSA, 25 mg

packaging

pack of 100

technique(s)

QuEChERS: suitable

centrifuge tube volume

2 mL

application(s)

food and beverages

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This Item
55176-U55173-U55172-U
Supelco

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55174-U

Supel QuE

Supelco

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55176-U

Supel QuE

Supelco

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55173-U

Supel QuE

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Supel QuE

composition

magnesium sulfate, 150 mg

composition

magnesium sulfate, 150 mg , Supelclean ENVI-Carb, 7.5 mg , Supelclean PSA, 25 mg

composition

Discovery® C18, 25 mg , magnesium sulfate, 150 mg , Supelclean PSA, 25 mg

composition

magnesium sulfate, 150 mg , Supelclean PSA, 25 mg

packaging

pack of 100

packaging

pack of 100

packaging

pack of 100

packaging

pack of 100

technique(s)

QuEChERS: suitable

technique(s)

QuEChERS: suitable

technique(s)

QuEChERS: suitable

technique(s)

QuEChERS: suitable

centrifuge tube volume

2 mL

centrifuge tube volume

2 mL

centrifuge tube volume

2 mL

centrifuge tube volume

2 mL

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

General description

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Legal Information

ENVI-Carb is a trademark of Sigma-Aldrich Co. LLC
Supel is a trademark of Sigma-Aldrich Co. LLC
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

13 - Non Combustible Solids

WGK

WGK 1

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


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25G
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1000309185

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Tsuyoshi Imazawa et al.
Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan, 46(6), 277-281 (2006-01-31)
An analytical method was developed for the determination of phenmedipham (PM) in agricultural products using reversed-phase high-performance liquid chromatography with UV detection. A sample was extracted with acetonitrile, and the acetonitrile layer was separated by salting-out. The acetonitrile phase was
Bing Shao et al.
Journal of AOAC International, 92(2), 604-611 (2009-06-03)
A sensitive analytical method has been developed and validated for simultaneous determination of 16 glucocorticoid (fluorometholone, flumethasone, triamcinolone, aldosterone, clobetasol propionate, methylprednisolone, fluocinolone acetonide, hydrocortisone, prednisone, dexamethasone, beclomethasone, prednisolone, budesonide, triamcinolone acetonide, fludrocortisone acetate, and cortisone) residues in pig tissues
Chang He et al.
Talanta, 164, 503-510 (2017-01-22)
Flame retardants are associated to numerous adverse health effects, can accumulate in humans and have been used intensively worldwide. Recently, dust has been identified as a major human exposure route for flame retardants. The aim of this study was to
Dajie Chen et al.
Se pu = Chinese journal of chromatography, 30(9), 896-902 (2013-01-05)
A high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/ MS) method was established for the determination of fungicide anilinopyrimidine residues including pyrimethanil, mepanipyrim, and cyprodinil in foodstuffs with series solid phase extraction (SPE). The food sample was first extracted with ethyl
U Führer et al.
Analytical and bioanalytical chemistry, 354(3), 333-343 (1996-01-01)
Halogenated anisoles (methyl-phenyl ethers) appear to be ubiquitous organic trace compounds in the environment. An analytical method is presented for analyzing the altogether 134 congeners of chloro-, bromo- and mixed bromochloro-anisoles on an isomer-specific basis in air. High volume sampling

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