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55288-U

Supelco

Supel™ QuE

PSA/C18 Tube, pack of 100, AOAC® 2007.01

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Synonym(s):
QuEChERS
NACRES:
NB.21

material

polypropylene tube

Quality Level

100

Agency

AOAC® 2007.01

product line

Supel™

composition

Discovery® DSC-18, 50 mg
magnesium sulfate, 150 mg
Supelclean PSA, 50 mg

packaging

pack of 100

technique(s)

QuEChERS: suitable

centrifuge tube volume

2 mL

matrix active group

C18 phase
PSA phase

application(s)

food and beverages

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This Item
55287-U55289-U55234-U
Supelco

Supelco

55288-U

Supel™ QuE

Supelco

Supelco

55287-U

Supel™ QuE

Supelco

Supelco

55289-U

Supel™ QuE

Supelco

Supelco

55234-U

Supel™ QuE

agency

AOAC® 2007.01

agency

AOAC® 2007.01

agency

AOAC® 2007.01

agency

AOAC® 2007.01

product line

Supel™

product line

-

product line

-

product line

Supel™

composition

Discovery® DSC-18, 50 mg

composition

magnesium sulfate, 150 mg , Supelclean PSA, 50 mg

composition

Discovery® DSC-18, 50 mg (;), ENVI-Carb, 50 mg , magnesium sulfate, 150 mg , Supelclean PSA, 50 mg

composition

magnesium sulfate, 6 g , sodium acetate, 1.5 g (Cat. No. 58750)

packaging

pack of 100

packaging

pack of 100

packaging

pack of 100

packaging

pk of 50

technique(s)

QuEChERS: suitable

technique(s)

QuEChERS: suitable

technique(s)

QuEChERS: suitable

technique(s)

QuEChERS: suitable

General description

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Legal Information

AOAC is a registered trademark of AOAC International
Discovery is a registered trademark of Sigma-Aldrich Co. LLC
Supel is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

13 - Non Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

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M Picot Groz et al.
The Science of the total environment, 493, 162-169 (2014-06-20)
The UV filters and musk fragrances have come into focus because these compounds are contained and increasingly used not only in sunscreen products but also in many products of daily use, such as cosmetics, skin creams, plastics or varnish. In
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
Yelena Sapozhnikova et al.
Analytica chimica acta, 758, 80-92 (2012-12-19)
A multi-class, multi-residue method for the analysis of 13 novel flame retardants, 18 representative pesticides, 14 polychlorinated biphenyl (PCB) congeners, 16 polycyclic aromatic hydrocarbons (PAHs), and 7 polybrominated diphenyl ether (PBDE) congeners in catfish muscle was developed and evaluated using
Maria Teresa Salles Trevisan et al.
Journal of chromatography. A, 1512, 98-106 (2017-07-20)
An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction
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Determination of Neonicotinoids in Honey using a Chromolith RP-18 HPLC column and UV Detection

Determination of Neonicotinoids in Honey using a Chromolith RP-18 HPLC column and UV Detection

Protocols

LC/MS/MS Analysis of Neonicotinoid Pesticides in Dandelion Blossoms on Ascentis® Express C18 after Dispersive SPE (QuEChERS) using Supel™ QuE

LC/MS/MS Analysis of Neonicotinoid Pesticides in Dandelion Blossoms on Ascentis® Express C18 after Dispersive SPE (QuEChERS) using Supel™ QuE

Banned and Other Neonicotinoids from Plant Material

On Friday, April 27, 2018, the European Union decided to ban the use of three neonicotinoid insecticides from use on field crops, having deemed them dangerous to bees. This application demonstrates the analysis of these banned compounds and others from dandelion blossoms using QuEChERS and LC-MS.

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Supel™ QuE Z-Sep Sorbents for QuEChERS

QuEChERs is a solid phase extraction (SPE) technique for sample preparation. Supelco's innovative Z-Sep and Z-Sep+ sorbents demonstrated here extract more fat and pigment than traditional PSA/C18 phases while showing greater analyte recovery and greater reproducibility.

Chromatograms

application for HPLCapplication for HPLC, application for SPE

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