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M-108

Supelco

MTBSTFA (with 1% t-BDMCS)

(with 1% t-BDMCS), ampule of 5 × 1 mL, analytical standard, Cerilliant®

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Synonym(s):
N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide with 1% tert-Butyldimethylchlorosilane, N-Methyl-N-tert-butyldimethylsilyltrifluoroacetamide, MTBSTFA + 1% TBDMSCl, Silylating mixture VI
Empirical Formula (Hill Notation):
C9H18F3NOSi
CAS Number:
Molecular Weight:
241.33
Beilstein/REAXYS Number:
3606546
MDL number:
PubChem Substance ID:

grade

analytical standard

Quality Level

reaction suitability

reagent type: derivatization reagent
reaction type: Acylations

packaging

ampule of 5 × 1 mL

manufacturer/tradename

Cerilliant®

technique(s)

gas chromatography (GC): suitable

application(s)

forensics and toxicology

format

neat

storage temp.

−20°C

SMILES string

CN(C(=O)C(F)(F)F)[Si](C)(C)C(C)(C)C

InChI

1S/C9H18F3NOSi/c1-8(2,3)15(5,6)13(4)7(14)9(10,11)12/h1-6H3

InChI key

QRKUHYFDBWGLHJ-UHFFFAOYSA-N

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This Item
009423759348.14219
vibrant-m

M-108

MTBSTFA (with 1% t-BDMCS)

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

technique(s)

-

technique(s)

-

format

neat

format

-

format

-

format

-

grade

analytical standard

grade

for GC derivatization

grade

-

grade

-

reaction suitability

reagent type: derivatization reagent
reaction type: Acylations

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

reaction suitability

-

reaction suitability

-

packaging

ampule of 5 × 1 mL

packaging

-

packaging

-

packaging

-

Legal Information

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany

pictograms

FlameExclamation mark

signalword

Warning

Hazard Classifications

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2

Storage Class

3 - Flammable liquids

wgk_germany

WGK 3

flash_point_f

113.0 °F - closed cup

flash_point_c

45 °C - closed cup


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Clayton B'Hymer et al.
Analytical and bioanalytical chemistry, 383(2), 201-209 (2005-09-15)
Several extraction and derivatization procedures were evaluated for the quantification of (2-methoxyethoxy)acetic acid (MEAA) in urine. MEAA is a metabolite and a biomarker for exposure to 2-(2-methoxyethoxy)ethanol, a glycol ether with widespread use in various industrial applications and the specific
José Angel Prieto et al.
Clinical biochemistry, 42(1-2), 125-128 (2008-11-11)
Evaluation of a GC-MS method using N-tert-butyldimethylsilyl-N-methyltrifluoroacetamide (MTBSTFA) as the silylating agent for GC-MS. Study of the stability of creatine and guanidinoacetate in urine. 22 urines were kept at RT, 4 degrees C and -30 degrees C for 15 days.
Paul L Wood et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 831(1-2), 313-319 (2006-01-13)
The GC-MS quantitation of a large number of neurochemicals utilizing a single derivatization step is not common but is provided by the reagent N-(tert-butyldimethylsilyl)-N-methyltrifluro-acetamide (MTBSTFA). Previous workers have utilized this derivative for GC-MS analyses of amino acids, carboxylic acids and
P Canosa et al.
Journal of chromatography. A, 1072(1), 107-115 (2005-05-11)
A solid-phase microextraction (SPME) method for the determination of triclosan, methyl triclosan, 2,4-dichlorophenol and 2,3,4-trichlorophenol (considered as possible triclosan metabolites) in water samples was optimised. Analytes were first concentrated on a SPME fibre, directly exposed to the sample, and then
Xiaowei Wang et al.
Journal of chromatography. A, 1216(35), 6267-6273 (2009-07-31)
A sample pretreatment method for the determination of 18 chlorophenols (CPs) in aqueous samples by derivatization liquid-phase microextraction (LPME) was investigated using gas chromatography-mass spectrometry. Derivatization reagent was spiked into the extraction solvent to combine derivatization and extraction into one

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