8.52124

Fmoc-Lys(Alloc)-OH

≥98.0% (HPLC), for peptide synthesis, Novabiochem^®

• 別名: Fmoc-Lys(Alloc)-OH
• 実験式（ヒル表記法）: C₂₅H₂₈N₂O₆
• CAS番号: 146982-27-6
• 分子量: 452.50
• MDL番号: MFCD00190872
• UNSPSCコード: 12352209
• NACRES: NA.22

特性

• product name: Fmoc-Lys(Alloc)-OH, Novabiochem^®
• 品質水準: 200
• 製品種目: Novabiochem^®
• アッセイ: ≥96.0% (acidimetric); ≥98% (TLC); ≥98.0% (HPLC)
• 形状: powder
• 反応適合性: reaction type: Fmoc solid-phase peptide synthesis
• メーカー／製品名: Novabiochem^®
• mp: 87-91 °C
• アプリケーション: peptide synthesis
• 官能基: amine
• 保管温度: 2-30°C
• InChI: 1S/C25H28N2O6/c1-2-15-32-24(30)26-14-8-7-13-22(23(28)29)27-25(31)33-16-21-19-11-5-3-9-17(19)18-10-4-6-12-20(18)21/h2-6,9-12,21-22H,1,7-8,13-16H2,(H,26,30)(H,27,31)(H,28,29)/t22-/m0/s1
• InChI Key: OJBNDXHENJDCBA-QFIPXVFZSA-N

詳細

詳細

Orthogonally-protected building block for the synthesis of branched and cyclic peptides and peptides modified at the Lys side chain by Fmoc SPPS. The Alloc group can be selectively removed in the presence of standard Fmoc- and t-butyl-based protecting groups by treatment with Pd(Ph₃P)₄/CHCl₃/AcOH/NMM.

Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS
Guide to Selection of Orthogonally -Protected Building Blocks for Fmoc SPPS

関連事項

Replaces: 04-12-1305

アナリシスノート

Color (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Enantiomeric purity: ≥ 99.5 % (a/a)
Optical rotation α 25/D (c=1 in DMF): -13.5 - -11.0 °
Purity (TLC(157A)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Assay (acidimetric): ≥ 96.0 %
Water (K. F.): ≤ 1.00 %

To see the solvent systems used for TLC of Novabiochem^® products please click here.

法的情報

Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany

安全性情報

• 保管分類コード: 11 - Combustible Solids
• WGK: WGK 3
• 引火点(°F): Not applicable
• 引火点(℃): Not applicable