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54281-U

Supelco

Supelclean Ultra 2400

volume 3 mL, pkg of 54

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Synonym(s):
Supelclean Ultra
NACRES:
NB.21

product line

Supelclean

Quality Level

composition

bed A, 270 mg (Supelclean PSA, Discovery® C18, and Spherical Carbon)
bed B, 225 mg (Z-Sep)

packaging

pkg of 54

technique(s)

solid phase extraction (SPE): suitable

volume

3 mL

matrix active group

C18 bonding
PSA bonding
carbon bonding

application(s)

food and beverages

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This Item
54332-U54216-U54341-U
Supelclean Ultra 2400 volume 3 mL, pkg of 54

Supelco

54281-U

Supelclean Ultra 2400

Supelclean™ EZ-POP NP volume 12 mL, pkg of 20

Supelco

54341-U

Supelclean EZ-POP NP

technique(s)

solid phase extraction (SPE): suitable

technique(s)

solid phase extraction (SPE): suitable

technique(s)

solid phase extraction (SPE): suitable

technique(s)

solid phase extraction (SPE): suitable

matrix active group

C18 bonding, PSA bonding, carbon bonding

matrix active group

aminopropyl phase, carbon phase

matrix active group

aminopropyl phase, carbon phase

matrix active group

C18 bonding phase, florisil bonding phase, zirconia bonding phase

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

application(s)

food and beverages

product line

Supelclean

product line

-

product line

-

product line

Supelclean

composition

bed A, 270 mg (Supelclean PSA, Discovery® C18, and Spherical Carbon)

composition

bed A, 500 mg (Supelclean ENVI-Carb), bed B, 500 mg (Supelclean LC-NH2)

composition

bed A, 500 mg (Supelclean ENVI-Carb), bed B, 500 mg (Supelclean LC-NH2)

composition

bed A, 1.25 g (Supelclean LC-Florisil®), bed b, 1.25 g (Z-Sep/C18)

General description

This multi-bed solid phase extraction (SPE) cartridge was designed for the cleanup of extracts of difficult matrices such as dry commodities (tea, spices, coffee, etc.) prior to pesticide residue analysis, typically performed by GC/MSMS and LC/MS/MS. These types of samples can contain pigments and oils, and may not be sufficiently cleaned using a standard QuEChERS cleanup.
The top bed consists of a mixture of PSA/C18 and a graphitized, spherical carbon. PSA removes acidic interferences, C18 retains some hydrophobic interferences, and carbon removes pigments. The variety of carbon used in this cartridge was engineered to remove sufficient pigmentation while allowing for better recoveries of compounds with planar structures. The bottom bed of the cartridge contains Z-Sep, which is a zirconia-coated silica. Z-Sep removes oily residues, and provides additional pigment removal.
The cartridge can be used for cleanup of acetonitrile extracts to be analyzed by either GC or HPLC.

Legal Information

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Pictograms

CorrosionExclamation mark

Signal Word

Danger

Hazard Statements

Hazard Classifications

Eye Dam. 1 - Skin Sens. 1

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


Certificates of Analysis (COA)

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T1503
Product Number
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25G
Pack Size/Quantity

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705578-5MG-PW

PL860-CGA/SHF-1EA

MMYOMAG-74K-13

1000309185

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Articles

Analysis of Pesticides in Turmeric Powder by LC/MS/MS and GC/MS/MS after Cleanup with Dual-Layer SPE Cartridge

Pesticide residue testing of turmeric and other (dried) spices is challenging due to their complex compositions and high matrix. An efficient SPE clean-up can be achieved by a new Dual-layer cartridge.

Analysis of Pesticide Residues in Ginger Powder Using QuEChERS Extraction and Clean-up with a Novel Dual Layer SPE Cartridge

The odor and pungency of ginger is due to the presence of terpenes, gingerols and shogaols. These compounds contribute to the highly complex matrix of ginger, which subsequently presents a challenge in low level analyses of contaminants. A novel 2-layer SPE cartridge efficiently reduces background for pesticide determination.

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

Contact Technical Service