G005864

HPLC Analysis of Triacylglycerols in Olive Oil on Discovery^® HS C18 after Sample Prep using Discovery^® DSC-Si (Propionitrile Mobile Phase, ELSD Detection)

application for HPLC

特性

• テクニック: HPLC: suitable
• 試験パラメータ: SPE tube/cartridge: Discovery DSC-Si, 1 gm/6 mL (52656-U); condition: 6 mL hexane; sample addition: 0.12 g oil in 0.5 mL hexane; elution: 10 mL hexane-diethyl ether 87-13 (v/v); eluate post-treatment: evaporation to dryness, reconstituted into 2 mL acetone; column: Discovery HS C18, 25 cm x 4.6 mm I.D., 5 μm particles (568523-U); mobile phase: propionitrile; flow rate: 1.5 mL/min; pressure: 1117 psi (77 bar); column temp.: 30 °C; detector: ELSD; injection: 5 μL
• 適合性: application for HPLC
• アプリケーション: food and beverages

詳細

アナリシスノート

Olive oil was pre-cleaned using Silica SPE, analyzed as 5% sample in acetone (w/v).

法的情報

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany

アナライト

LLL
OOO