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Merck
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주요 문서

SU860097

Supelco

Headspace vial, screw top, rounded bottom (vial only)

volume 20 mL, clear glass vial, thread for 18, O.D. × H 22.5 mm × 75.5 mm, pkg of 100 ea

동의어(들):

Screw cap rounded bottom headspace vial

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About This Item

UNSPSC 코드:
41122001
NACRES:
NB.11

material

clear glass vial
round bottom

특징

closure type screw top vial

포장

pkg of 100 ea

O.D. × H

22.5 mm × 75.5 mm

용적

20 mL

피팅

thread for 18

호환성

for use with CTC PAL (Varian, Gerstel, Atas, Shimadzu)

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일반 설명

These vials require a special cap with an 18 mm thread. The standard 18-400 threaded caps will not fit this vial. The part numbers for caps that are available for these vials are SU860101(with PTFE/silicone, 1.3 mm thick), SU860102 (with PTFE/butyl, 1.6 mm thick), and SU860103 (with PTFE/silicone, 1.5 mm thick). These caps are made from stainless steel and are magnetic.

애플리케이션

Headspace vial may be used for the following:
  • In the determination of partition coefficient of ethyl acetate in water at 0° C from independent analyses of the total amount of ethyl acetate present in the vial, by automatic equilibrium headspace gas chromatography and vapor phase calibration (VPC).
  • It may be used in the analysis of volatile polar residual solvents present in pharmaceutical products, during development and optimisation of headspace SPME method by GC-MS.
  • It may also be used in the isotopic analysis of 18O in the leaf water of C3 and C4 grasses, during establishing a grassland signature in veins, as it was found that grasses with different photosynthetic pathway have different interveinal differences.
  • It may also find application, in investigating metabolism by Pseudomonas fluorescens of volatile haloaliphatic hydrocarbons like 1,2-dichloroethane and 1,2-dichloropropane, which are some of the major contaminants of underground aquifers.

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시험 성적서(COA)

Lot/Batch Number

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이 제품을 이미 가지고 계십니까?

문서 라이브러리에서 최근에 구매한 제품에 대한 문서를 찾아보세요.

문서 라이브러리 방문

Determination of partition coefficients by automatic equilibrium headspace gas chromatography by vapor phase calibration.
Welter KBC and Bichler C.
Chromatographia, 34 (5-8), 235-240 (1992)
B R Helliker et al.
Proceedings of the National Academy of Sciences of the United States of America, 97(14), 7894-7898 (2000-07-08)
We show that 18O evaporative enrichment of bulk leaf water in grass species can be significantly more enriched than predicted by the Craig-Gordon model, with C4 grasses considerably more enriched than C3 grasses. Our results suggest that the unanticipated 18O
P A Vandenbergh et al.
Applied and environmental microbiology, 54(10), 2578-2579 (1988-10-01)
A Pseudomonas fluorescens strain designated PFL12 was isolated from soil and water that were contaminated with various chloroaliphatic hydrocarbons. The isolate was able to metabolize 1,2-dichloroethane, 1,1,2-trichloroethane, 1,2-dichloropropane, 2,2-dichloropropane, and trichloroethylene.
C C Camarasu
Journal of pharmaceutical and biomedical analysis, 23(1), 197-210 (2000-07-18)
A solid-phase microextraction (SPME) method has been developed and optimized for the polar residual solvent determination in pharmaceutical products. Five different polymer-coated fibers were investigated and the Carboxen/polydimethylsiloxane was found to be the most sensitive for all components. Two Headspace

프로토콜

물에 함유된 VOC의 측정을 위해 GC/MS와 조합한 HS-SPME의 고성능, 신뢰성 및 재현성은 실험실간 시험에서 입증되었습니다. HS-SPME를 이용한 새로운 ISO 17943은 민감도와 선택성에서 이 측정의 기존 공식 방법을 개선하였습니다.

High performance, reliability, and reproducibility of HS-SPME in combination with GC/MS for the determination of VOCs in water was proven in an interlaboratory trial. The new ISO 17943 using HS-SPME is an improvement on existing official methods for this determination in terms of sensitivity and selectivity.

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