GC Analysis of Alkylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec^® CHIRALDEX^™ B-TA

column

Astec CHIRALDEX B-TA, 30 m x 0.25 mm I.D., 0.12 μm (73023AST)

gradient

80 °C, 2 °C/min to 110 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 30 psi

injection

0.6 μL, 80:1 split

sample

2.5 mg/mL each racemate in methanol (N-TFA derivatives)