GC Analysis of 1-Phenylethanol Enantiomers on Astecยฎ CHIRALDEXโข B-PM
Materials
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CONDITIONS
column
Astec CHIRALDEX B-PM, 30 m x 0.25 mm I.D., 0.12 μm (76023AST)
oven
120 ยฐC
inj. temp.
250 ยฐC
detector
FID, 250 ยฐC
carrier gas
helium, 24 psi
injection
1 μL, 80:1 split
sample
3 mg/mL in methanol
peak 1: R(+)-1-phenylethanol
peak 2: S(-)-1-phenylethanol
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Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC